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Sound technical content, curated with aloha by
Ted Mooney, P.E. RET
Pine Beach, NJ
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Problems activating Electroless Nickel plated parts




Q. Hi all, I have some Aluminium parts that have been plated using Electroless Nickel.
The Nickel has been buffed to a very high shine so that it resembles a mirror but I cannot get the nickel to activate.
I have tried nickel activator and SS activator but nothing.
Has anyone any ideas what I can do to activate my part?

Vicki Phillips
hobbyist, product designer - Ayr, Scotland
July 27, 2008



simultaneous replies

A. Firstly, make sure your surfaces are absolutely clean and have no surface contamination on them. It is important that you are exposing the nickel metal and have removed all other coatings. Next, connect the workpiece to the negative power supply and the positive side to a piece of metal. Ideally use nickel, but if you haven't any, use a piece of copper wire or something. Put the workpiece and piece of metal in the electroless nickel solution and quickly turn on the power - you only need a low current density (say 1 ASF) for less than a minute. You will start to see gas bubbles coming off the workpiece - then your electroless nickel will start to work. As soon as it does start, remove your metal wire and turn off the power

trevor crichton
Trevor Crichton
R&D practical scientist
Chesham, Bucks, UK
July 31, 2008


A. First, you have to get all of the polish off. That can be a trick because you do not know what was used, so how do you take it off.
30%^ nitric acid by volume and 1.5% by weight hydrofluoric acid will work well. Stay in the dip till you see a flow of very tiny bubbles start and then rinse and plate very rapidly.

James Watts
- Navarre, Florida
July 30, 2008



simultaneous replies

OOPS, My post should have been 30% nitric acid and 1.5% hydrofluoric acid. The HF is extremely dangerous so think twice about using it.

James Watts
- Navarre, Florida
July 31, 2008



Hi, an easy way I have found to re-activate electroless nickel is to tungsten etch it for about 1 minute , then back in the nickel solution ...

Hope this helps .

Jay Smith
- UK
July 31, 2008


Q. Jay, I have never heard of a tungsten etch on this side of the puddle. Please, what is it?

James Watts
- Navarre, Florida
August 1, 2008




Q. I have a similar but more complex problem. I have some nickel-iron parts which have electroless nickel plating (15-20 microns). I need to strip the plating off but normal strippers, as you would expect, eat the base material too. Just to add to the difficulty, these parts have been furnaced but thankfully are clean. Is there a way the electroless can be reactivated without affecting the base material?

James Mayle
- United Kingdom
April 2, 2015




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